4.2.3.9 6.3 7.5 - 4.2.3.9 7.5 - assay at 4.2.3.9 7.5 - activity assay 4.2.3.9 7.5 - preparative scale incubation, 48 h 4.2.3.9 7.6 - assay at 4.2.3.9 8 - recombinant enzyme, HEPES buffer